COMBINED COMPENDIUM OF FOOD ADDITIVE …
GENERAL METHODS APPEARANCE AND PHYSICAL PROPERTIES Boiling Point and Distillation Range. The following method employs 100 ml of sample. In cases where it is necessary or would be desirable to use a smaller sample, the method of McCullough et al. [J. Chem. Ed. 47, 57 (1970)], which employs only 50 µl of sample, may be used.